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1 article(s) from Manzoli, Maela

Reaction of oxiranes with cyclodextrins under high-energy ball-milling conditions

László Jicsinszky,
Federica Calsolaro,
Katia Martina,
Fabio Bucciol,
Maela Manzoli and
Giancarlo Cravotto

Beilstein J. Org. Chem. 2019, 15, 1448–1459, doi:10.3762/bjoc.15.145

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Scheme 1: The reaction of CDs with oxiranes.

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Figure 1: Jar-temperature changes during the reaction of 1,2-propylene oxide and cyclodextrins in the presenc...

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Figure 2: Comparative SEM pictures of a β-CD bead and β-CDP (20 mmol, Table 3, entry 10).

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Figure 3: Comparison of β-CDP (Table 3, entry 9) and γ-CDP (Table 3, entry 12) prepared in a ball mill on 2 mmol scale.

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Figure 4: Normalised particle-size distribution of insoluble CD polymers (entries 9, 10, and 12 of Table 3).

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Figure 5: UV–vis spectra and adsorption isotherm of the insoluble β-CDP polymer in 10 ml 0.050 mM MO solution...

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Figure 6: UV–vis spectral changes of 0.050 mM MO solution by GPTS-β-CD (left) and GPTS-γ-CD (right), as prepa...

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Figure 7: UV–vis spectral changes of 0.050 mM MO solution by GPTS-β-CD (left) and GPTS-γ-CD (right), as prepa...

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Published 01 Jul 2019

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